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A project log for Improve the Haber process

See if ultrasonic cavitation can be used to fixate atmospheric Nitrogen less expensively than the Haber process.

peter-walshPeter Walsh 09/09/2015 at 20:110 Comments

.) Reaction chamber v3.0

.) Complete list of components, $50 total cost

.) Trying a "bubble plate"

.) Capturing bubbles in a standing wave works... 'sorta


Reaction chamber, v3.0

The tube holder for the reaction chamber was a bit unwieldy, so I added mounting tabs to the back plate of the reaction chamber and changed the lid as needed.

The new version holds the tube firmly in place, and has extra mounting holes for future use.

The chamber layout is now based on a specific thickness and vendor for acrylic (Plaskolite, 5.75mm), so it's easy for anyone to cut out and assemble.

To use a different thickness you'll have to resize the tabs and notches - if I get time after the contest maybe I'll make a parametric program that generates the pattern based on the thickness the user has available.


Completed list of components

The Hackaday.io project components are complete and final (I hope!). All chips are listed, except I glossed over minor electronic things like passives and XOR gates and such.

The final list of components are:

With parts from eBay the whole system costs around $50, not counting the 2 ATX supplies.


Bubble Plate

Holding a bubble at the end of the gas inlet tube is proving to be problematic. There's a fine line between having a bubble and either a) no bubble, or b) releasing a bubble.

I want the bubble held stationary, so I machined a concave depression into the head of a small bolt. This will attach to the gas inlet tube and serve as a catcher plate for released bubbles. This way I can position the bubble with the plate and not have to worry about keeping it at the end of the tube.

UPDATE: It works well enough, but isn't sturdily mounted to the gas tube - it keeps flipping over. Oh well - it's a nut & bolt, shouldn't be to hard to figure out a mounting bracket.


Capturing bubbles in a standing wave

Thinking about ultrasonic levitation, I got to wondering if the reverse was possible. Can a standing wave capture a bubble under water?

It turns out it can. I was able to get a bubble to "hover" above a reflecting plate for about a minute before it wandered off.

Once.

I don't have a picture because it's hard to place the bubble in just the right position. Several times I positioned the bubble, only to have it fly away a few seconds later. It was definitely hovering for those few seconds, however.

This really isn't the right horn or the right way to do this. If I get some time I'll play around some more later. Maybe a horn with a slight depression would arrange the energy to better capture the bubble.

The speed of sound in water is 1482 m/s, the frequency is 28,000 hz, so the half wavelength is 26.46 mm.

Position a flat horn any multiple of this distance over the reflecting plate to get standing waves.

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